Ethylene ¯ame Synthesis of Well-aligned Multi-walled Carbon Nanotubes
نویسندگان
چکیده
A stainless steel grid baked by a propane±air premixed ¯ame had iron, chromium and nickel oxide deposits on the grid surface. With this grid, entangled and curved shape multi-walled carbon nanotubes (MWNTs) were harvested from an ethylene±air diusion ¯ame with yield rate of 3 mg/min. Nitrogen addition to the ¯ame was found to straighten the entangled tubes probably by lowering the ¯ame temperature. A cobalt-electrodeposited stainless steel grid was ®nally applied to the nitrogen-diluted ethylene diusion ¯ame; well-aligned and well-graphitized carbon nanotubes consisting of 20 nm diameter and 10 lm long element tubes were obtained.
منابع مشابه
Synthesis of Some New Disperse Dyes-multi Walled Carbon Nanotubes Adducts and Impact Analysis of Substituents
We have reported here a simple, low cost preparation of four new adducts from some anthraquinone disperse dyes with functionalized multi-walled carbon nanotubes in the presence of azochromophore. The structural differences between the final products are evaluated by visual dispersion test, UV-Vis Spectroscopy, Fourier transforms infrared, Raman, nuclear magnetic resonance and thermal gravimetri...
متن کاملEffect of ion bombardment on the synthesis of vertically aligned single-walled carbon nanotubes by plasma-enhanced chemical vapor deposition.
The synthesis of vertically aligned single-walled carbon nanotubes (VA-SWNTs) by plasma-enhanced chemical vapor deposition (PECVD) was achieved at 500-600 °C, using ethylene as the carbon source and 1 nm Fe film as the catalyst. For growth of high-quality VA-SWNTs in a plasma sheath, it is crucial to alleviate the undesirable ion bombardment etching effects by the optimization of plasma input p...
متن کاملMulti-walled carbon nanotubes supported palladium nanoparticles: Synthesis, characterization and catalytic activity towards methanol electro oxidation in alkaline media
Palladium nanoparticles supported on multi-walled carbon nanotubes (Pd/MWCNTs) have been synthesized using a modified polyol reduction method and its performance in methanol oxidation reactions has evaluated. The morphology of palladium on MWCNTs was characterized by scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The catalytic performance of synthesized catalyst ...
متن کاملFunctionalized Carbon Nanotubes Produced by APCVD using Camphor
A simple chemical vapor deposition technique at atmospheric pressure (APCVD) is adopted to synthesize the aligned arrays of functionalized multi-walled carbon nanotubes (AMWCNTs) without using any carrier gas, at 230◦C, 750◦C and 850 ◦C. Camphor (C10H16O) is used as carbon source because this botanical hydrocarbon is chip and abundant which convert the CVD technique to a green method for produc...
متن کاملNovel and Simple Synthesis Method for Submillimeter Long Vertically Aligned Single-Walled Carbon Nanotubes by No-Flow Alcohol Catalytic Chemical Vapor Deposition
Using a conventional thermal chemical vapor deposition (CVD) system, ethanol vapor was enclosed in a reactor, i.e., no flow, with Co/Mo dip-coated quartz substrates to synthesize submillimeter long vertically aligned single-walled carbon nanotube (SWNT) films successfully. The no-flow CVD method yielded an increase in film thickness of up to 0.11 mm compared with the normal flowing gas method f...
متن کامل